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Effect of Ti addition on microstructure and high-temperature soft magnetic properties of nanocrystalline (Fe0.9Co0.1)72.7Al0.8Si13.5B9Cu1Nb3 alloy
Physica B: Condensed Matter ( IF 2.8 ) Pub Date : 2020-11-11 , DOI: 10.1016/j.physb.2020.412701
Qian-qian Hao , Zhi Wang , Xian-hua Li , Yan Zhang , Rui-min Shi

The crystallization behavior and microstructure of (Fe0.9Co0.1)72.7Al0.8Si13.5B9-xCu1Nb3Tix(x = 0,1,2) alloys were analyzed by the differential scanning calorimetry (DSC) and X-ray diffractometry (XRD). The soft magnetic properties of alloys after thermal treatment were studied by the temperature dependence of initial permeability (μi-T curves). Experimental results show that the proper addition of Ti can decrease the onset temperature of primary crystallization Tx1 for precipitating soft magnetic phase from 506 °C for x = 0–487 °C for x = 1 and increase the onset temperature of second crystallization Tx2 from 669 °C for x = 0–703 °C for x = 2. The extended onset temperature of second crystallization Tx2 of 703 °C and crystallization temperature interval ΔTx of 199 °C make the 650oC-annealed (Fe0.9Co0.1)72.7Al0.8Si13.5B7Cu1Nb3Ti2 alloy exhibit superior magnetic softness at room- and high-temperatures. And the 610oC-annealed (Fe0.9Co0.1)72.7Al0.8Si13.5B8Cu1Nb3Ti1 alloy shows improved high-temperature magnetic softness at 450–650 °C with respect to Ti-free (Fe0.9Co0.1)72.7Al0.8Si13.5B9Cu1Nb3 alloy.



中文翻译:

钛添加对纳米晶(Fe 0.9 Co 0.172.7 Al 0.8 Si 13.5 B 9 Cu 1 Nb 3合金的组织和高温软磁性能的影响

 用差示扫描量热法(DSC)和X-射线衍射仪分析了(Fe 0.9 Co 0.172.7 Al 0.8 Si 13.5 B 9- x Cu 1 Nb 3 Ti xx = 0,1,2)合金的结晶行为和显微组织。射线衍射仪(XRD)。热处理后合金的软磁特性通过初始磁导率的温度依赖性的研究(μ-T曲线)。实验结果表明,适当添加Ti可降低主结晶开始温度Ť X1从506℃下析出软磁性相X  = 0-487℃,X  = 1,并增加第二结晶起始温度Ť X2从669℃,X  = 0-703℃,X  = 2扩展第二次结晶的开始温度Ť X2的703℃,结晶化温度间隔ΔT X的199℃使650 Ô C-退火(铁0.90.172.7的Al 0.8的Si 13.57的Cu 1 Nb的3的Ti 2该合金在室温和高温下均表现出优异的磁柔软性。610 o C退火(Fe 0.9 Co 0.172.7 Al 0.8 Si 13.5 B 8 Cu 1 Nb 3 Ti 1合金相对于无Ti(Fe 0.9 Co 0.172.7 Al 0.8 Si 13.5 B 9 Cu 1 Nb 3合金。

更新日期:2021-01-18
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