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Solvent-free synthesis of cyclic polycaprolactone catalysed by MOF-derived ZnO/NCs catalysts
European Polymer Journal ( IF 5.8 ) Pub Date : 2021-01-01 , DOI: 10.1016/j.eurpolymj.2020.110127 Farah Naz , Matteo Ciprian , Bibimaryam Mousavi , Somboon Chaemchuen , Meifang Zhu , Shilin Yan , Francis Verpoort
European Polymer Journal ( IF 5.8 ) Pub Date : 2021-01-01 , DOI: 10.1016/j.eurpolymj.2020.110127 Farah Naz , Matteo Ciprian , Bibimaryam Mousavi , Somboon Chaemchuen , Meifang Zhu , Shilin Yan , Francis Verpoort
Abstract For the first time, ZnO dispersed in an N-doped carbon matrix (ZnO/NCs) was derived from the controlled thermal treatment of Zn-DABCO and utilized as a robust heterogeneous catalyst for the polymerization of e-caprolactone. The as-prepared ZnO/NCs catalysts were characterized using TEM, SEM, Raman spectroscopy, XPS, XRD, TPD and N2 adsorption. The catalyst displayed excellent activity towards the e-caprolactone polymerization reaction, following the trend, Zn/NC-1000
中文翻译：
MOF衍生的ZnO/NCs催化剂催化无溶剂合成环状聚己内酯
摘要 ZnO 分散在 N 掺杂的碳基体 (ZnO/NCs) 中，首次源自 Zn-DABCO 的受控热处理，并将其用作稳定的多相催化剂，用于 e-己内酯的聚合。使用 TEM、SEM、拉曼光谱、XPS、XRD、TPD 和 N2 吸附对制备的 ZnO/NCs 催化剂进行表征。该催化剂对ε-己内酯聚合反应表现出优异的活性，顺应趋势，Zn/NC-1000
更新日期：2021-01-01
中文翻译：
MOF衍生的ZnO/NCs催化剂催化无溶剂合成环状聚己内酯
摘要 ZnO 分散在 N 掺杂的碳基体 (ZnO/NCs) 中，首次源自 Zn-DABCO 的受控热处理，并将其用作稳定的多相催化剂，用于 e-己内酯的聚合。使用 TEM、SEM、拉曼光谱、XPS、XRD、TPD 和 N2 吸附对制备的 ZnO/NCs 催化剂进行表征。该催化剂对ε-己内酯聚合反应表现出优异的活性，顺应趋势，Zn/NC-1000
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