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Preparation of strontium doped mesoporous ZnO nanoparticles to investigate their dye degradation efficiency
Nano Express ( IF 2.7 ) Pub Date : 2020-10-30 , DOI: 10.1088/2632-959x/abc393
Balvinder Kumar 1, 2 , Suresh Kumar 1, 2 , Virender Singh 1, 2 , Anil Vohra 1, 2 , Nikhil Chauhan 1, 2 , Rajesh Goyal 2
Affiliation  

Mesoporous strontium doped ZnO nanoparticles are synthesized as photocatalyst by using zinc nitrate hexahydrate, surfactant P123, strontium nitrate hexahydrate via the hydrothermal process. X-ray diffraction (XRD), UV-visible spectroscopy (UV), Fourier transform infrared (FTIR), Photoluminescence (PL), Energy-dispersive x-ray (EDX), Scanning electron microscopy (SEM), Transmission Electron Microscopy (TEM), and Brunauer–Emmett–Teller (BET) characterizations are used for the analysis of all the samples. XRD spectra disclose the disparity in the crystal size 14.98 to 22.74 nm. The study of UV spectroscopy revealed the energy bandgap difference between 3.3–2.92 eV. PL spectroscopy shows the effect of doping on the electron-hole recombination rate of the sample. FTIR analysis has utilized to determine the functional groups such as –OH, C=O=C, and –C–O present in the sample. EDX spectra show the elemental compositions of the sample. SEM images show the agglomerated morphology and TEM...

中文翻译:

锶掺杂介孔ZnO纳米粒子的制备及其对染料降解的研究

利用硝酸锌六水合物,表面活性剂P123,硝酸锶六水合物经水热法合成了介孔锶掺杂的ZnO纳米粒子作为光催化剂。X射线衍射(XRD),紫外可见光谱(UV),傅立叶变换红外(FTIR),光致发光(PL),能量色散X射线(EDX),扫描电子显微镜(SEM),透射电子显微镜(TEM) )和Brunauer-Emmett-Teller(BET)表征用于所有样品的分析。XRD光谱揭示了晶体尺寸为14.98至22.74nm的差异。紫外光谱研究表明,能带隙在3.3–2.92 eV之间。PL光谱显示掺杂对样品的电子-空穴复合速率的影响。FTIR分析已用于确定官能团,例如–OH,C = O = C,样品中存在–C–O。EDX光谱显示了样品的元素组成。SEM图像显示了聚集的形态和TEM ...
更新日期:2020-10-30
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