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Butylamine-resadiye bentonite composite characterization
Spectroscopy Letters ( IF 1.7 ) Pub Date : 2020-10-12 , DOI: 10.1080/00387010.2020.1832530
E. Koksal 1 , B. Afsin 1 , A. Tabak 2 , B. Caglar 3
Affiliation  

Abstract The acid activation process increased the specific surface area of raw Resadiye bentonite (33.5 m2/g) by ∼ 4-fold whereas the interaction with n-butylamine caused a surface area reduction of acid-activated bentonite by 40% along with the broadening of the Si-O stretching peak at 1041 cm−1 and the decrease of the d001 value from 14.5 to 13.5 Å. The thermal analysis data confirmed the stability of the mesoporous n-butylamine/acid-activated bentonite composite up to 499 °C which was followed by the cleavage of the interlayer n-butylamine species between 500 and 700 °C.

中文翻译:

丁胺-resadiye膨润土复合材料表征

摘要 酸活化过程使原始 Resadiye 膨润土 (33.5 m2/g) 的比表面积增加了约 4 倍,而与正丁胺的相互作用导致酸活化膨润土的表面积减少了 40%,同时加宽了Si-O 拉伸峰在 1041 cm-1,d001 值从 14.5 降低到 13.5 Å。热分析数据证实了介孔正丁胺/酸活化膨润土复合材料在高达 499 °C 时的稳定性,然后在 500 到 700 °C 之间裂解层间正丁胺物质。
更新日期:2020-10-12
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