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Synthesis of 2,3-Diphenylacrolein Acetals
Russian Journal of General Chemistry ( IF 0.9 ) Pub Date : 2020-10-12 , DOI: 10.1134/s1070363220090248
G. N. Sakhabutdinova , G. Z. Raskilʼdina , S. S. Zlotskii

Abstract

Linear acetals have been synthesized by decomposition trans- and cis-1,1-dichloro-2,3-diphenylcyclopropanes in the presence of aliphatic alcohols (ethanol and butan-1-ol). The reactivities of pure trans- and cis-stilbenes and styrene toward dichlorocarbene have been compared. The structure of the isolated compounds was determined by NMR and GC/MS.



中文翻译:

2,3-二苯基丙烯醛缩醛的合成

摘要

线性缩醛已经通过分解合成反式-和CIS中的脂族醇(乙醇和丁-1-醇)的存在下-1,1-二氯-2,3- diphenylcyclopropanes。纯的反应性反式和--stilbenes朝二氯卡宾苯乙烯进行了比较。分离的化合物的结构通过NMR和GC / MS确定。

更新日期:2020-10-12
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