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Microstructure and Mechanical Properties of BCC-FCC Eutectics in Ternary, Quaternary and Quinary Alloys From the Al-Co-Cr-Fe-Ni System
Frontiers in Materials ( IF 2.6 ) Pub Date : 2020-08-27 , DOI: 10.3389/fmats.2020.567793
Daniel Röhrens , Niloofar Navaeilavasani , Oleg Stryzhyboroda , Fabian Swientek , Paul Pavlov , Dirk Meister , Amber Genau , Ulrike Hecht

This study aimed at understanding the structure and properties of dual-phase eutectics in ternary, quaternary, and quinary alloys of the Al-Co-Cr-Fe-Ni system. The alloys at case were i) Ni48Fe34Al18, ii) Ni44Fe20Cr20Al16, and iii) Ni34.4Fe16.4Co16.4Cr16.4Al16.4. Samples in the form of cylindrical bars, diameter 10 mm × 150 mm, were produced by arc melting and suction casting from pure elements (>99.9 wt%). Bridgman solidification at low growth velocity was used to produce additional samples with large eutectic spacing and lamellae thickness of the two phases body-centered cubic (BCC)-B2 and face-centered cubic (FCC) in order to facilitate phase characterization by energy-dispersive X-ray analysis (scanning electron microscopy/energy-dispersive spectroscopy) and nano-indentation. In agreement with thermodynamic calculations, each of the phases was found to be multi-component and contain all alloying elements in distinct amounts. The mechanical properties of the individual phases were analyzed in relation to their composition using nano-indentation experiments. These measurements revealed some insights into “high-entropy effects” and their contribution to the elastoplastic response to indentation loading. Further analysis focused on as-cast as well as heat-treated samples comprising phase fraction measurements, micro-indentation, and miniature testing in three-point bending configuration. For optimum heat treatment conditions, a good balance of strength and ductility was obtained for each of the investigated alloys. Further work is necessary in order to assess their capability as structural materials.



中文翻译:

Al-Co-Cr-Fe-Ni体系三元,四元和五元合金中BCC-FCC共晶的微观结构和力学性能

这项研究旨在了解Al-Co-Cr-Fe-Ni系统的三元,四元和五元合金中的双相共晶结构和性能。情况下的合金为i)Ni 48 Fe 34 Al 18,ii)Ni 44 Fe 20 Cr 20 Al 16和iii)Ni 34.4 Fe 16.4 Co 16.4 Cr 16.4 Al 16.4。通过电弧熔化和吸铸,由纯元素(> 99.9重量%)制成直径为10 mm×150 mm的圆柱状样品。使用低生长速度的Bridgman固化来生产具有大共晶间距和两相薄板厚度的两个样品,体心立方(BCC)-B2和面​​心立方(FCC)以便通过能量分散来表征相X射线分析(扫描电子显微镜/能量分散光谱)和纳米压痕。与热力学计算一致,发现每个相都是多组分的,并且包含不同量的所有合金元素。使用纳米压痕实验分析了各个相的机械性能及其组成。这些测量结果揭示了对“高熵效应”及其对压痕载荷弹塑性响应的贡献的一些见解。进一步的分析集中在铸态和热处理样品上,包括相分数测量,微压痕和三点弯曲配置的微型测试。为了获得最佳的热处理条件,每种研究合金均获得了强度和延展性的良好平衡。为了评估其作为结构材料的能力,需要做进一步的工作。为了获得最佳的热处理条件,每种研究合金均获得了强度和延展性的良好平衡。为了评估其作为结构材料的能力,需要做进一步的工作。为了获得最佳的热处理条件,每种研究合金均获得了强度和延展性的良好平衡。为了评估其作为结构材料的能力,需要做进一步的工作。

更新日期:2020-10-07
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