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Structural evolution and hardness of molybdenum deformed by high pressure torsion at 573 K
International Journal of Refractory Metals & Hard Materials ( IF 4.2 ) Pub Date : 2020-09-28 , DOI: 10.1016/j.ijrmhm.2020.105389
T.M. Gapontseva , M.V. Degtyarev , L.M. Voronova , T.I. Chashchukhina , V.P. Pilyugin

The structural evolution of initial single-crystal {110} Мо during high pressure torsion at 573 К has been investigated by scanning and transmission electron microscopy. Two stages of the structure formation have been found. At the first stage, the single-crystal transforms into the polycrystal with a {110} weak texture. At the second stage (е ≥ 4), the average grain size is constant (about 0.5 μm) due to dynamic recrystallization. An increase in the gradient of an internal grain orientation (grain orientation spread) after the maximally-achieved true strain (е = 7.1) indicates the high defectiveness of the dynamically-recrystallized structure and, as a result, a rise in the hardness of Mo.



中文翻译:

573 K下高压扭转变形钼的结构演变和硬度

通过扫描和透射电子显微镜研究了在573К高压扭转期间初始单晶{110}Мо的结构演变。已经发现结构形成的两个阶段。在第一阶段,单晶转变为具有弱{110}织构的多晶。在第二阶段(≥4),由于动态再结晶,平均晶粒尺寸恒定(约0.5μm)。在达到最大真实应变(е  = 7.1 )之后,内部晶粒取向的梯度(晶粒取向扩展)的增加表明动态再结晶组织的缺陷率很高,结果,Mo的硬度增加。

更新日期:2020-10-05
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