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Synthesis of siloxane nanogel with phenylboronic functional groups
Phosphorus, Sulfur, and Silicon and the Related Elements ( IF 1.4 ) Pub Date : 2020-09-25 , DOI: 10.1080/10426507.2020.1804142 Sergey A. Milenin 1 , Fedor V. Drozdov 1 , Ivan B. Meshkov 1 , Aziz M. Muzafarov 1
Phosphorus, Sulfur, and Silicon and the Related Elements ( IF 1.4 ) Pub Date : 2020-09-25 , DOI: 10.1080/10426507.2020.1804142 Sergey A. Milenin 1 , Fedor V. Drozdov 1 , Ivan B. Meshkov 1 , Aziz M. Muzafarov 1
Affiliation
Abstract In this work, a siloxane nanogel containing phenyl borate functional groups was obtained consistently by condensation of the sodium salt of methyltriethoxysilane in acetic acid and further functionalization with 4,4,5,5-tetramethyl-2-styryl-1,3,2-dioxaborolane (St-BPin) by hydrosilylation reaction. The obtained nanogel was investigated by NMR and IR spectroscopy, element analysis, and GPC. GRAPHICAL ABSTRACT
中文翻译：
具有苯基硼官能团的硅氧烷纳米凝胶的合成
摘要 在这项工作中，通过甲基三乙氧基硅烷的钠盐在乙酸中缩合并进一步与 4,4,5,5-四甲基-2-苯乙烯基-1,3,2 -二氧杂硼烷 (St-BPin) 通过氢化硅烷化反应。通过核磁共振和红外光谱、元素分析和 GPC 研究了获得的纳米凝胶。图形概要
更新日期：2020-09-25
中文翻译：
具有苯基硼官能团的硅氧烷纳米凝胶的合成
摘要 在这项工作中，通过甲基三乙氧基硅烷的钠盐在乙酸中缩合并进一步与 4,4,5,5-四甲基-2-苯乙烯基-1,3,2 -二氧杂硼烷 (St-BPin) 通过氢化硅烷化反应。通过核磁共振和红外光谱、元素分析和 GPC 研究了获得的纳米凝胶。图形概要
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