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Performance analysis of VPSA process for separating N2O from adipic acid tail gas
Separation and Purification Technology ( IF 8.1 ) Pub Date : 2020-09-25 , DOI: 10.1016/j.seppur.2020.117750
Tongbo Wu , Zhaoyang Niu , Li Feng , Xiuxin Yu , Bing Liu , Donghui Zhang

A four-bed and six-bed vacuum pressure swing adsorption (VPSA) process with silical gel were proposed to separate and purify N2O from adipic acid tail gas (N2O/N2/O2 = 0.3933/0.5657/0.041 mol%) in nylon plants and then the N2O could be rectified to produce ultra-high purity N2O. The four-bed VPSA process was developed to study the relationship between vacuum pressure and simulation performances, the resulting recovery of N2O exceeds 90% with a purity over 95%. Meanwhile, the six-bed process was designed to explore the effects of vacuum and feed flow rate. The results indicated that a 95.55% purity N2O stream is attained for a process N2O recovery of 97.45%, when the feed flow rate was 1434.8 NL/s and vacuum pressure was 0.247 bar and N2O energy was 4.95 KJ/mol N2O respectively.



中文翻译:

VPSA工艺从己二酸尾气中分离N 2 O的性能分析

提出了采用硅胶的四床六床真空变压吸附(VPSA)工艺从己二酸尾气中分离纯化N 2 O(N 2 O / N 2 / O 2  = 0.3933 / 0.5657 / 0.041 mol %)在尼龙植物则n 2 O的程序可能整流以产生超高纯ñ 2 O的四床VPSA方法的开发是为了研究得到的N个恢复真空压力和仿真性能之间的关系,2 ö超过90%,纯度超过95%。同时,设计了六床工艺来研究真空和进料流速的影响。结果表明纯度为95.55%的N 2当进料流速为1434.8 NL / s,真空压力为0.247 bar,N 2 O能量为4.95 KJ / mol N 2 O时,获得的O物流的N 2 O回收率为97.45%。

更新日期:2020-10-11
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