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In-situ observation of nucleation, growth and interaction of deformation-induced α″ martensite in metastable Ti–10V–2Fe–3Al
Materials Science and Engineering: A ( IF 6.1 ) Pub Date : 2020-09-21 , DOI: 10.1016/j.msea.2020.140237
Frank Niessen , Azdiar A. Gazder , David R.G. Mitchell , Elena V. Pereloma

Microstructure evolution, dominated by the formation of deformation-induced α martensite during the 3-point bending of a metastable β Ti–10V–2Fe–3Al alloy containing 5% α, was observed in-situ using forward-scatter electron imaging and electron backscattering diffraction. α plates nucleated heterogeneously from {580}α habit planes at α-β interfaces and triggered the nucleation of additional α plates at the advancing interface during growth and upon impingement with high-angle boundaries. Further thickening of the impinged α plates led to a build-up of strain energy which induced {130}31¯0α twinning within obstacle-forming α plates. Until now, this twinning system was observed in Nb and Ta alloyed Ti shape memory alloys only. This in-situ study is also the first to document the activation of {130}31¯0α twinning by α impingement in a metastable β matrix. The first forming variants were {011}α compound twin-related variant pairs, each forming from up to two individual habit planes. These variant pairs were consistently predicted by determining the grain-average stress with finite element analysis and computing the available work from the transformation strain of the α variants. At higher indenter loads, grains that were unfavourably oriented to martensite formation accommodated the local stress by forming aggregates of different α variants, obeying either {111}α type I or 211α type II twin relationships. Scanning transmission electron microscopy revealed α substructures comprising columnar domains oriented perpendicular to the habit plane along with the absence of lattice invariant deformation. The growth of α plates involved ledge formation at α-β interfaces.



中文翻译:

形变诱导的形核,生长和相互作用的原位观察 α'' 亚稳态Ti–10V–2Fe–3Al中的马氏体

微观结构演变,主要由形变诱发的形成 α'' 亚稳三点弯曲过程中的马氏体 β 含5%的Ti-10V-2Fe-3Al合金 α,使用前向散射电子成像和电子反向散射衍射原位观察。 α'' 异质核板 {580}α'' 习惯于 α--β 接口并触发了附加的成核 α''在生长过程中以及受到大角度边界撞击时,在前进界面处的板块。进一步加厚α'' 板导致应变能的积累,从而引起 {130}31个¯0α'' 在障碍物形成中孪生 α''盘子。迄今为止,仅在Nb和Ta合金化的Ti形状记忆合金中观察到这种孪生系统。这项原位研究也是第一个记录激活{130}31个¯0α'' 结对 α'' 冲击在亚稳态 β矩阵。第一个成型变体是{011}α''复合的双胞胎相关变体对,每个变体对最多由两个独立的习惯平面组成。通过使用有限元分析确定晶粒平均应力,并根据合金的转变应变计算可用功,可以一致地预测这些变体对。α''变体。在较高的压头载荷下,不利于马氏体形成的晶粒通过形成不同的聚集体来适应局部应力α'' 变体,服从 {111}α'' I型或 211α''II型双胞胎关系。扫描透射电子显微镜显示α''子结构包含垂直于习性平面定向的柱状畴,并且不存在晶格不变变形。的成长α'' 板块涉及壁架形成 α''--β 接口。

更新日期:2020-09-21
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