Materials Science and Engineering: A ( IF 6.1 ) Pub Date : 2020-09-21 , DOI: 10.1016/j.msea.2020.140237 Frank Niessen , Azdiar A. Gazder , David R.G. Mitchell , Elena V. Pereloma
Microstructure evolution, dominated by the formation of deformation-induced martensite during the 3-point bending of a metastable Ti–10V–2Fe–3Al alloy containing 5% , was observed in-situ using forward-scatter electron imaging and electron backscattering diffraction. plates nucleated heterogeneously from habit planes at - interfaces and triggered the nucleation of additional plates at the advancing interface during growth and upon impingement with high-angle boundaries. Further thickening of the impinged plates led to a build-up of strain energy which induced twinning within obstacle-forming plates. Until now, this twinning system was observed in Nb and Ta alloyed Ti shape memory alloys only. This in-situ study is also the first to document the activation of twinning by impingement in a metastable matrix. The first forming variants were compound twin-related variant pairs, each forming from up to two individual habit planes. These variant pairs were consistently predicted by determining the grain-average stress with finite element analysis and computing the available work from the transformation strain of the variants. At higher indenter loads, grains that were unfavourably oriented to martensite formation accommodated the local stress by forming aggregates of different variants, obeying either type I or type II twin relationships. Scanning transmission electron microscopy revealed substructures comprising columnar domains oriented perpendicular to the habit plane along with the absence of lattice invariant deformation. The growth of plates involved ledge formation at - interfaces.
中文翻译:
形变诱导的形核,生长和相互作用的原位观察 亚稳态Ti–10V–2Fe–3Al中的马氏体
微观结构演变,主要由形变诱发的形成 亚稳三点弯曲过程中的马氏体 含5%的Ti-10V-2Fe-3Al合金 ,使用前向散射电子成像和电子反向散射衍射原位观察。 异质核板 习惯于 -- 接口并触发了附加的成核 在生长过程中以及受到大角度边界撞击时,在前进界面处的板块。进一步加厚 板导致应变能的积累,从而引起 在障碍物形成中孪生 盘子。迄今为止,仅在Nb和Ta合金化的Ti形状记忆合金中观察到这种孪生系统。这项原位研究也是第一个记录激活 结对 冲击在亚稳态 矩阵。第一个成型变体是复合的双胞胎相关变体对,每个变体对最多由两个独立的习惯平面组成。通过使用有限元分析确定晶粒平均应力,并根据合金的转变应变计算可用功,可以一致地预测这些变体对。变体。在较高的压头载荷下,不利于马氏体形成的晶粒通过形成不同的聚集体来适应局部应力 变体,服从 I型或 II型双胞胎关系。扫描透射电子显微镜显示子结构包含垂直于习性平面定向的柱状畴,并且不存在晶格不变变形。的成长 板块涉及壁架形成 -- 接口。