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Nanomechanical properties of hardened 60NiTi
Materials Science and Engineering: A ( IF 6.1 ) Pub Date : 2020-09-16 , DOI: 10.1016/j.msea.2020.140284
Charles Miller , Christopher DellaCorte , Min Zou

The nanomechanical properties of hardened 60NiTi were studied using nanoindentation. The hardened 60NiTi consists of two regions: the NiTi + Ni4Ti3 region, which is composed of a B2 NiTi matrix and nanoscale Ni4Ti3 precipitates, and the globular Ni3Ti precipitates. Blind nanoindentation was first performed on 60NiTi using a diamond Berkovich without differentiating the regions. The two regions were then selectively indented using a diamond cube corner nanoindenter. The results show that the elastic modulus and hardness of the NiTi + Ni4Ti3 region were similar to those of bulk 60NiTi. The Ni3Ti phase was found to have an elastic modulus that is more than double that of bulk 60NiTi and the NiTi + Ni4Ti3 region. The hardness was also found to be significantly higher. This study not only provides the first quantitative measurements of the mechanical properties of Ni3Ti precipitates within 60NiTi but also suggests that the presence of large amounts of easily imaged Ni3Ti could serve as a good indication of reduced amounts of Ni4Ti3, which could lead to lower overall hardness of the material.



中文翻译:

硬化60NiTi的纳米力学性能

使用纳米压痕研究了硬化的60NiTi的纳米力学性能。硬化的60NiTi由两个区域组成:由B2 NiTi基体和纳米级Ni 4 Ti 3沉淀物组成的NiTi + Ni 4 Ti 3区域,以及球状Ni 3 Ti沉淀物。首先使用金刚石Berkovich在60NiTi上进行盲纳米压痕,而无需区分区域。然后使用菱形立方角纳米压头选择性地压入两个区域。结果表明,NiTi + Ni 4 Ti 3区的弹性模量和硬度与块状60NiTi相似。镍3发现Ti相的弹性模量是整体60NiTi和NiTi + Ni 4 Ti 3区的弹性模量的两倍以上。还发现硬度明显更高。这项研究不仅提供了对60NiTi内Ni 3 Ti析出物力学性能的首次定量测量,而且表明大量易成像的Ni 3 Ti的存在可以很好地表明Ni 4 Ti 3含量的减少,这可能会导致材料的整体硬度降低。

更新日期:2020-09-23
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