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Synthesis of N , N '-Disubstituted Dithiooxamide Derivatives by the Modified Willgerodt–Kindler Reaction
Russian Journal of Organic Chemistry ( IF 0.8 ) Pub Date : 2020-06-26 , DOI: 10.1134/s1070428020050097 T. N. Ponomareva , E. V. Eliseenkov , A. A. Petrov , V. P. Boyarskii
中文翻译:
修饰的Willgerodt–Kindler反应合成N,N'-二取代的二硫代乙酰胺衍生物
更新日期:2020-06-26
Russian Journal of Organic Chemistry ( IF 0.8 ) Pub Date : 2020-06-26 , DOI: 10.1134/s1070428020050097 T. N. Ponomareva , E. V. Eliseenkov , A. A. Petrov , V. P. Boyarskii
Abstract
The conditions of the reaction of trichloroethylene with sulfur and amines were optimized (the modified Willgerodt–Kindler reaction). The reaction of tetrachloroethylene with sulfur and some basic primary and secondary amines of the aliphatic series in DMF under mild conditions leads to N,N'-disubstituted dithiooxamides in 30–70% yields and with a 100% conversion of tetrachloroethylene.中文翻译:
修饰的Willgerodt–Kindler反应合成N,N'-二取代的二硫代乙酰胺衍生物