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A one-step facile route synthesis of copper oxide/reduced graphene oxide nanocomposite for supercapacitor applications
Journal of Experimental Nanoscience ( IF 2.6 ) Pub Date : 2018-12-07 , DOI: 10.1080/17458080.2018.1542512
Suresh Sagadevan 1, 2 , Zaira Zaman Chowdhury 3 , Mohd. Rafie Bin Johan 3 , Fauziah Abdul Aziz 1 , Emee Marina Salleh 1 , Anil Hawa 1 , Rahman F. Rafique 4
Affiliation  

In this research, a one step, facile route has been undertaken to synthesise copper oxide/reduced graphene oxide (CuO/rGO) nanocomposites. X-ray powder diffraction analysis (XRD) was carried out to identity the crystalline structure and phase of the synthesised sample. Elemental analysis and surface morphological features were analysed using EDX and FESEM Images. Particle size as well as the shape of the as prepared composite was observed from HR-TEM images. Raman spectra illustrated the peak of the individual composite materials. The electrochemical properties of the prepared nanocomposite were investigated. The dielectric behaviour of the sample including dielectric constant, dielectric loss and AC conductivity was measured at various frequency levels. Temperature was varied accordingly to observe the effect of temperature on the dielectric properties of the sample.



中文翻译:

超级电容器应用的氧化铜/还原氧化石墨烯纳米复合材料的一步式简便路线合成

在这项研究中,已经采取了一种简单的方法来合成氧化铜/还原氧化石墨烯(CuO / rGO)纳米复合材料。进行X射线粉末衍射分析(XRD)以鉴定合成样品的晶体结构和相。使用EDX和FESEM图像分析元素分析和表面形态特征。从HR-TEM图像观察颗粒尺寸以及所制备的复合物的形状。拉曼光谱说明了各个复合材料的峰。研究了制备的纳米复合材料的电化学性能。在各种频率水平下测量样品的介电性能,包括介电常数,介电损耗和交流电导率。

更新日期:2018-12-07
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