Journal of the European Ceramic Society ( IF 5.8 ) Pub Date : 2020-09-05 , DOI: 10.1016/j.jeurceramsoc.2020.09.005 Philippe Garcia , Audrey Miard , Thomas Helfer , Jean-Baptiste Parise , Xavière Iltis , Guy Antou
We report a set of compression test experiments carried out on sintered uranium dioxide at 1500 C, at constant strain rates and under controlled oxygen partial pressures. The macroscopic data indicate an initial strain hardening stage followed by a quasi steady-state period during which changes in the stress level are sluggish. The data are further interpreted in a continuum mechanics, finite strain framework, in both one and two-dimensional geometries, whence stress and oxygen partial pressure exponents of the creep law are estimated. The stress exponent is indicative of power-law creep. The oxygen partial pressure exponent is consistent with a strain-rate limited by vacancy mediated self-diffusion of the slowest moving ion, suggesting a climb-controlled recovery process. Some samples are further characterized using SEM/EBSD which reveals signs of plastic deformation typical of recovery creep. The effect of oxygen pressure upon microstructure is discussed.
中文翻译:
氧分压对多晶二氧化铀中位错蠕变的影响
我们报告了在1500烧结二氧化铀上进行的一组压缩测试实验 C,在恒定应变速率和受控氧分压下。宏观数据表明,在初始应变硬化阶段之后是准稳态阶段,在此期间应力水平的变化缓慢。在一维和二维几何结构中,在连续力学有限应变框架中进一步解释数据,据此估算蠕变律的应力和氧分压指数。应力指数表示幂律蠕变。氧分压指数与应变速率一致,该速率受空位介导的最慢运动离子的自我扩散限制,表明爬升控制的恢复过程。一些样品使用SEM / EBSD进行了进一步表征,显示出典型的恢复蠕变塑性变形迹象。