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Studies of Influence of ZrO 2 Nanoparticles on Reinforced Conducting Polymer and Their Optical, Thermal and Electrochemical Properties
Journal of Inorganic and Organometallic Polymers and Materials ( IF 3.9 ) Pub Date : 2020-09-02 , DOI: 10.1007/s10904-020-01730-3
F. Z. Hammadi , M. S. Belardja , M. Lafjah , A. Benyoucef

Nanocomposites based on zirconium oxide, modified with o-Aminosulfanilic acid have been synthetized. Samples have been prepared by chemical polymerization. The resulting products were fully characterized by XPS, XRD, FTIR, SEM and UV–vis spectroscopies which have shown that nanocomposites have been carried out. Essentially, this work represents an efficacious way of setting the thermal and optical properties of the synthesized hybrid materials, prepared by adjusted the ZrO2 quantities during chemical synthesis; the interfacial interactions between poly(oASA) and ZrO2 have been confirmed by different physio-chemical analysis. The poly(oASA)@ZrO2 (3%) sample proved a good electroactivity response where achieve two oxidation peaks and three reduction peaks at 502, 849, 743, 669 and 388 mV, respectively.



中文翻译:

ZrO 2纳米粒子对增强导电聚合物的影响及其光学,热和电化学性能的研究

合成了基于氧化锆的纳米复合材料,并用邻氨基氨基磺酸改性。样品已经通过化学聚合制备。通过XPS,XRD,FTIR,SEM和UV-vis光谱对得到的产品进行了充分表征,表明已进行了纳米复合材料的制备。本质上,这项工作代表了一种通过在化学合成过程中调节ZrO 2量来制备合成杂化材料的热和光学性质的有效方法。聚(oASA)和ZrO 2之间的界面相互作用已通过不同的理化分析得到证实。聚(oASA)@ZrO 2 (3%)样品证明具有良好的电活性,在502、849、743、669和388 mV处分别达到两个氧化峰和三个还原峰。

更新日期:2020-09-02
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