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Utility of N-Bromosuccinimide–Water Combination as a Green Reagent for Synthesis of N,S-Heterocycles and Dithiocarbamates from Styrenes
Synlett ( IF 1.7 ) Pub Date : 2020-08-28 , DOI: 10.1055/s-0040-1707258
Firouz Matloubi Moghaddam 1 , Mehri Goudarzi
Affiliation  

An efficient and unprecedented green protocol has been developed for the synthesis of N,S-heterocycles from styrenes and alkyl dithiocarbamates with high to excellent yields. The reaction of primary or secondary amines, CS2, and styrenes was carried out in water in the presence of a catalytic amount of an inorganic base. All products were made by using an N-bromosuccinimide–H2O combination as a green and inexpensive reagent.

中文翻译:

N-溴代琥珀酰亚胺-水组合作为绿色试剂用于从苯乙烯合成 N,S-杂环和二硫代氨基甲酸酯的效用

已开发出一种高效且前所未有的绿色方案,用于从苯乙烯和二硫代氨基甲酸烷基酯合成 N,S-杂环,收率高至极好。在催化量的无机碱存在下,伯胺或仲胺、CS2和苯乙烯的反应在水中进行。所有产品均使用 N-溴代琥珀酰亚胺-H2O 组合作为绿色且廉价的试剂制成。
更新日期:2020-08-28
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