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A laboratory transmission diffraction Laue setup to evaluate single-crystal quality
Journal of Applied Crystallography ( IF 5.2 ) Pub Date : 2020-07-08 , DOI: 10.1107/s1600576720006317
Alexiane Arnaud , Wijdène Guediche , Clément Remacha , Edward Romero , Henry Proudhon

A scanning laboratory Laue transmission setup is developed to probe extended quasi-monocrystalline samples. Orientation mapping is achieved by controlling the collimation of the incident beam and scanning the position of the specimen. An automated indexing algorithm for transmission Laue patterns is presented, together with a forward simulation model adapted for a laboratory setup. The effect of the main parameters of the system is studied with the aim of achieving exposure times of the order of one second. Applications are presented to probe the orientation of an extended part and detect disoriented regions within the bulk. Finally, the analysis of diffraction spot shapes shows that the misorientation within the illuminated volume can be measured, and a new method is proposed to evaluate its complete mean lattice rotation tensor.

中文翻译:

用于评估单晶质量的实验室透射衍射劳厄装置

开发了扫描实验室劳厄透射装置来探测扩展的准单晶样品。定向映射是通过控制入射光束的准直和扫描试样的位置来实现的。介绍了传输劳厄模式的自动索引算法,以及适用于实验室设置的前向模拟模型。研究系统主要参数的影响,目的是实现一秒量级的曝光时间。提出了用于探测延伸部分的方向并检测块体内方向混乱的区域的应用程序。最后,衍射光斑形状的分析表明可以测量被照射体积内的取向差,并提出了一种评估其完整平均晶格旋转张量的新方法。
更新日期:2020-07-08
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