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Process intensification of Three Phase Partition for extraction of custard apple seed oil using Microwave Pretreatment
Chemical Engineering and Processing: Process Intensification ( IF 4.3 ) Pub Date : 2020-08-14 , DOI: 10.1016/j.cep.2020.108095
Dhanashree C. Panadare , Virendra K. Rathod

The application of microwave was observed to be an emerging intensification tool in the field of extraction. A recent study in extraction revels the rising prospectus of the microwave as an integrated unit operation with Three Phase Partitioning (TPP). This work aims to determine the best mode of microwave application for TPP assisted extraction of oil from custard apple seeds, which has significant industrial potential as a biopesticide. A maximum oil extraction yield of 33.23 (w/w) % was obtained by opting microwave pre-treatment assisted Three Pase partitioning (MPTPP) with 120 W applied power for 60 s as optimized parameters. Parameters affecting TPP, such as salt concentration, aqueous to t-butanol ratio, and slurry to t-butanol ratio, were also optimized as 45% (w/v), 1:2 (v/v) and 1:10 respectively. Also, MPTPP was observed to extract 18.46 (w/w) % of protein along with the maximum oil extraction. In MPTPP, the yield of oil was improved by 1.13-fold than the conventional method, and the process time was reduced by 2.5 times than TPP.



中文翻译:

微波预处理三相分区强化奶油苹果籽油的提取工艺。

微波的应用被认为是提取领域中新兴的强化工具。一项最新的提取研究显示,将微波作为具有三相分割(TPP)的集成单元操作,正在兴起。这项工作旨在确定微波应用的最佳方式,用于TPP辅助从奶油苹果种子中提取油,这具有作为生物农药的巨大工业潜力。通过以120 W的施加功率选择60 s的微波预处理辅助三步分配(MPTPP)作为优化参数,可获得33.23(w / w)%的最大采油率。影响TPP的参数(例如盐浓度,水与叔丁醇的比例以及浆液与叔丁醇的比例)也分别优化为45%(w / v),1:2(v / v)和1:10。另外,观察到MPTPP提取了18。46(w / w)%的蛋白质以及最大的油提取率。在MPTPP中,油的收率比常规方法提高了1.13倍,并且处理时间比TPP减少了2.5倍。

更新日期:2020-09-14
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