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Structural, dielectric and nonlinear properties of potassium hydrogen oxalate-trihydroxy boron (KHC2O4 B(OH)3) single-crystal
Journal of Solid State Chemistry ( IF 3.2 ) Pub Date : 2020-08-06 , DOI: 10.1016/j.jssc.2020.121642
D.S. Ajisha , R. Ezhil Vizhi

A metal-organic compound of potassium hydrogen oxalate-trihydroxy boron was grown by solution growth method. The solubility curve validates the positive temperature gradient of the compound. The polythermal method was used for the determination of the metastable zone width of the compound. The structure of the grown crystal was analyzed through single-crystal XRD. The occurrence of different functional groups within the sample was explained with the help of FTIR analysis. The optical analysis was carried out and the optical band gap energy of the compound was calculated. The third-order nonlinearity of the compound was analyzed with the help of the Z-scan method. The impedance analyzer was employed to analyze the value of dielectric loss and constant of the crystal.



中文翻译:

草酸氢钾-三羟基硼(KHC 2 O 4 B(OH)3)单晶的结构,介电和非线性性质

通过溶液生长法生长草酸氢钾-三羟基硼的金属有机化合物。溶解度曲线验证了化合物的正温度梯度。多热法用于确定化合物的亚稳区宽度。通过单晶XRD分析生长的晶体的结构。借助FTIR分析解释了样品中不同官能团的出现。进行光学分析并计算化合物的光学带隙能。借助Z扫描法分析了该化合物的三阶非线性。使用阻抗分析仪分析介电损耗值和晶体常数。

更新日期:2020-08-06
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