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Handy Soft Jet Plasma as an Effective Technique for Tailored Preparation of ZnS Nanomaterials and Shape Dependent Antibacterial Performance of ZnS
Journal of Industrial and Engineering Chemistry ( IF 5.9 ) Pub Date : 2020-10-01 , DOI: 10.1016/j.jiec.2020.07.042
Antony Ananth , Ihn Han , Mahmuda Akter , Jin-Hyo Boo , Eun Ha Choi

Abstract In this study, zinc sulphide nanomaterial (ZnS NM) powders were prepared with the assistance of an atmospheric pressure soft jet plasma (APPJ) device. Regular approaches to ZnS preparation mainly resulted in aggregated powders, thus plasma methods were investigated to obtain controlled morphological structures. The APPJ plasma-assisted ZnS exhibited unique surface architectures, such as nanorods, layers and spherical aggregates, that were controllably obtained by changing the reactant concentration and type of precursor. The prepared ZnS showed good thermal stability by no changes in its composition up to 400 °C. The APPJ plasma-assisted ZnS showed sphalerite and wurtzite crystal structures and resulted in excellent chemical purity. The simple and handy APPJ plasma method shows good potential for shape-controlled ZnS NMs preparation without addition of surfactant chemicals, mechanical stirring, external heating or any other tedious procedures. This capability showcases the scientific and technological merit of this technique. The prepared ZnS NMs were utilized as antibacterial agents and evaluated the activity using three techniques against the human pathogens of E. coli, S. aureus and K. pneumoniae. The ZnS NMs showed effective concentration and shape-dependent activity when used as an antibacterial material.

中文翻译:

方便的软喷射等离子体作为一种有效的技术,用于定制 ZnS 纳米材料的制备和 ZnS 的形状相关抗菌性能

摘要 在这项研究中,在常压软射流等离子体 (APPJ) 装置的帮助下制备了硫化锌纳米材料 (ZnS NM) 粉末。ZnS 制备的常规方法主要导致聚集的粉末,因此研究了等离子体方法以获得受控的形态结构。APPJ 等离子体辅助 ZnS 表现出独特的表面结构,如纳米棒、层和球形聚集体,这些结构是通过改变反应物浓度和前体类型可控地获得的。制备的 ZnS 表现出良好的热稳定性,其成分在 400 °C 下没有变化。APPJ 等离子体辅助 ZnS 显示出闪锌矿和纤锌矿晶体结构,并具有优异的化学纯度。简单方便的 APPJ 等离子体方法显示出良好的形状控制 ZnS NMs 制备潜力,无需添加表面活性剂化学品、机械搅拌、外部加热或任何其他繁琐的程序。这种能力展示了这种技术的科学和技术价值。制备的 ZnS NMs 用作抗菌剂,并使用三种技术评估其对大肠杆菌、金黄色葡萄球菌和肺炎克雷伯氏菌的人类病原体的活性。当用作抗菌材料时,ZnS NMs 显示出有效的浓度和形状依赖性活性。制备的 ZnS NMs 用作抗菌剂,并使用三种技术评估其对大肠杆菌、金黄色葡萄球菌和肺炎克雷伯氏菌的人类病原体的活性。当用作抗菌材料时,ZnS NMs 显示出有效的浓度和形状依赖性活性。制备的 ZnS NMs 用作抗菌剂,并使用三种技术评估其对大肠杆菌、金黄色葡萄球菌和肺炎克雷伯氏菌的人类病原体的活性。当用作抗菌材料时,ZnS NMs 显示出有效的浓度和形状依赖性活性。
更新日期:2020-10-01
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