Photochemical synthesis of tungsten pentafluoride, WF5,Zeitschrift für anorganische und allgemeine Chemie

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Photochemical synthesis of tungsten pentafluoride, WF5
Zeitschrift für anorganische und allgemeine Chemie ( IF 1.1 ) Pub Date : 2020-06-18 , DOI: 10.1002/zaac.202000177
Riane Stene _{1,

2} , Benjamin Scheibe ₁ , Sergei I. Ivlev ₁ , Antti J. Karttunen ₃ , Winfried Petry ₂ , Florian Kraus ₁

Affiliation

A new synthetic route for the synthesis of WF5 utilizing a mercury photosensitized reduction of tungsten hexafluoride with H2 is described. Crystals of WF5 were studied using single-crystal X-ray diffraction, resulting in the first-reported crystal structure of WF5. Powder X-ray diffraction studied at room-temperature showed the compound was phase-pure. The IR spectrum of WF5 was re-

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