Titanium carbosilicide is synthesized by the method of spark plasma sintering (SPS) from a powder mixture of plain elements (Ti, Si, C). The stages of the synthesis process are considered, i.e., pressing of the powder mixture, melting of the constituents, chemical reactions, and phase transformations. The materials synthesized at 1000, 1300, 1500 and 1600°C are studied by the methods of phase, diffraction, and microscopic x-ray spectrum analysis. It is shown that 1600°C is a critical temperature causing total disintegration of titanium carbosilicide in the material.

中文翻译：

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通过火花等离子烧结 (SPS) 从普通元素合成碳硅化钛的工艺阶段

碳硅化钛是由普通元素（Ti、Si、C）的粉末混合物通过放电等离子烧结 (SPS) 方法合成的。考虑合成过程的各个阶段，即粉末混合物的压制、成分的熔化、化学反应和相变。通过相、衍射和显微 X 射线光谱分析方法研究了在 1000、1300、1500 和 1600°C 下合成的材料。结果表明，1600°C 是导致材料中碳硅化钛完全分解的临界温度。