Visible-Light Photoredox-Catalyzed Amidation of Benzylic Alcohols.,The Journal of Organic Chemistry

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Visible-Light Photoredox-Catalyzed Amidation of Benzylic Alcohols.
The Journal of Organic Chemistry ( IF 3.3 ) Pub Date : 2020-07-14 , DOI: 10.1021/acs.joc.0c01320
Silvia Gaspa ₁ , Andrea Farina ₁ , Mariella Tilocca ₁ , Andrea Porcheddu ₂ , Luisa Pisano ₁ , Massimo Carraro ₁ , Ugo Azzena ₁ , Lidia De Luca ₁

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A new photocatalyzed route to amides from alcohols and amines mediated by visible light is presented. The reaction is carried out in ethyl acetate as a solvent. Ethyl acetate can be defined a green and bio-based solvent. The starting materials such as the energy source are easily available, stable, and inexpensive. The reaction has shown to be general and high yielding.

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