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Range-by-Range Calculations of Absorption Coefficients as a Method for Increasing the Accuracy of Electron Probe Microanalysis
Journal of Analytical Chemistry ( IF 1.1 ) Pub Date : 2020-07-07 , DOI: 10.1134/s106193482005010x
Yu. G. Lavrent’ev , L. V. Usova , M. Yu. Lavrent’ev , N. S. Karmanov

Abstract

To increase the accuracy of electron probe microanalysis, it was proposed to calculate absorption coefficients range-by-range, with selecting an optimum calculation method for each absorption range. The approach was implemented in the analysis of rock-forming minerals using the PAP correction method. Calculations of absorption coefficients in the region below the K-edge were performed using the PAP method and, in K–L1 range, by the Heinrich method with certain refinements. A series of natural minerals with high iron (and zinc) contents were used for refinement. Practical tests confirmed the expediency and reliability of the range-by-range calculation of absorption coefficients.


中文翻译:

吸收系数的按距离计算,作为提高电子探针显微分析精度的一种方法

摘要

为了提高电子探针显微分析的准确性,提出了逐个范围地计算吸收系数,并为每个吸收范围选择最佳的计算方法。该方法是在使用PAP校正方法分析成岩矿物中实施的。在K边缘以下区域的吸收系数的计算是使用PAP方法进行的,在K–L 1范围内,通过Heinrich方法进行了某些改进。使用了一系列铁(和锌)含量高的天然矿物进行精炼。实际测试证实了吸收系数逐段计算的便利性和可靠性。
更新日期:2020-07-07
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