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Investigation of Microwave Processing Parameters on Development of Ni-40Cr 3 C 2 Composite Clad and Their Characterization
Metallurgical and Materials Transactions A ( IF 2.2 ) Pub Date : 2020-05-25 , DOI: 10.1007/s11661-020-05832-y
Jonty Mago , Sandeep Bansal , Dheeraj Gupta , Vivek Jain

The chromium carbide (Cr3C2)-reinforced Ni-based composite clad on austenitic stainless steel (SS-316) substrate was successfully developed by the microwave cladding route after optimizing process parameters (Power: 900 Watt, Exposure Time: 380 seconds). Clads were developed at 2.45 GHz frequency in a domestic microwave oven. The developed composite clad has been examined for metallurgical and mechanical properties. The investigation was carried out by using scanning electron microscopy (SEM) equipped with a backscatter electron detector, energy dispersive spectroscopy (EDS) for elemental analysis, and X-ray diffractometry (XRD) for phase analysis and their quantification and Vicker’s microhardness tester for microhardness. Clads of thickness 600 µm were successfully developed, which are free from visible pores and all types of cracks (interfacial or solidification cracks). The porosity analysis was carried out by using ASTM B-276 standard, and results reveal that porosity is less than 2 pct. The average microhardness of the developed clad is observed 605 ± 80 HV0.3. The developed clad was three times harder than the substrate (SS-316). The various intermetallic (Ni3Fe, Cr3Si, and Ni2Si) and different carbides (Cr7C3, NiC, Ni3C, SiC, and Cr3Ni2SiC) phases were observed through XRD examination. The distribution of intermetallic and various hard carbide phases in the clad has a direct influence on hardness and increases hardness at great extent.



中文翻译:

Ni-40Cr 3 C 2复合熔覆层形成过程的微波工艺参数研究及表征

优化工艺参数(功率:900瓦特,曝光时间:380秒),通过微波熔覆工艺成功开发了奥氏体不锈钢(SS-316)基底上的碳化铬(Cr 3 C 2)增强镍基复合涂层。 。包层是在家用微波炉中以2.45 GHz频率开发的。已对开发的复合覆层进行了冶金和机械性能检查。使用配备了背向散射电子检测器的扫描电子显微镜(SEM),用于元素分析的能量色散光谱(EDS)和用于相分析及其定量的X射线衍射仪(XRD)以及用于显微硬度的维氏显微硬度测试仪进行了研究。厚度为600 µ的包层m已成功开发,没有可见的孔洞和所有类型的裂纹(界面裂纹或凝固裂纹)。孔隙率分析是使用ASTM B-276标准进行的,结果表明孔隙率小于2 pct。观察到的复合层的平均显微硬度为605±80 HV 0.3。显影后的覆层比基材(SS-316)坚硬三倍。各种金属间化合物(Ni 3 Fe,Cr 3 Si和Ni 2 Si)和不同的碳化物(Cr 7 C 3,NiC,Ni 3 C,SiC和Cr 3 Ni 2通过XRD检查观察到SiC)相。包层中金属间和各种硬质合金相的分布对硬度有直接影响,并在很大程度上增加了硬度。

更新日期:2020-07-02
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