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Effect of annealing in tuning magnetic hyperthermic efficiency of MWCNT/CoFe 2 O 4 nanocomposites
Journal of Physics D: Applied Physics ( IF 3.1 ) Pub Date : 2020-06-28 , DOI: 10.1088/1361-6463/ab8de5
Papori Seal 1 , C Borgohain 2 , Nibedita Paul 1 , P D Babu 3 , J P Borah 1
Affiliation  

Annealing of a magnetic nanostructure is expected to not only change morphological features but also magnetic properties and hence magnetic hyperthermia applications. Using a simple co-precipitation method, annealed and non-annealed MWCNT/CoFe 2 O 4 nanocomposites have been synthesized, as confirmed by phases depicted in XRD. Here, a comparative study of morphological features, magnetic properties and heat dissipation capability of as-synthesized samples has been done. Transmission electron microscopy and scanning electron microscopy images reveal the agglomerated nature of the nanostructure. A visible shift in peak position of FTIR spectroscopy and Raman shift for annealed MWCNT/CoFe 2 O 4 nanocomposites from that of non-annealed MWCNT/CoFe 2 O 4 nanocomposites implies change in the vibrational features. As evident from vibrating sample magnetometer, coercivity and saturation magnetization increases for annealed MWCNT/CoF...

中文翻译:

退火对调节MWCNT / CoFe 2 O 4纳米复合材料磁热效率的影响

磁性纳米结构的退火不仅会改变形态特征,而且还会改变磁性,从而改变磁性热疗的应用范围。使用简单的共沉淀方法,已合成退火和未退火的MWCNT / CoFe 2 O 4纳米复合材料,这已通过XRD中描述的相证实。在此,对合成样品的形态特征,磁性能和散热能力进行了比较研究。透射电子显微镜和扫描电子显微镜图像揭示了纳米结构的团聚性质。与未退火的MWCNT / CoFe 2 O 4纳米复合材料相比,退火的MWCNT / CoFe 2 O 4纳米复合材料的FTIR光谱峰值位置和拉曼位移可见变化,这意味着振动特征发生了变化。
更新日期:2020-06-29
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