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Application of a Novel Ti/nanoSnO 2 -α-Fe 2 O 3 Anode for the Electro-Catalytic Degradation of Dye Pollutant: Optimization of Operational Parameters by Central Composite Design
Journal of The Electrochemical Society ( IF 3.1 ) Pub Date : 2020-06-25 , DOI: 10.1149/1945-7111/ab9d63
Fatemeh Mirzaei Abdoulyousefi , Farideh Nabizadeh Chianeh , Alireza Asghari

Electrochemical degradation of Acid Yellow 3 dye (AY3) in aqueous solution was investigated over a novel Ti/nanoSnO 2 -α-Fe 2 O3 electrode ssuccessfully fabricated by the cathodic electrophoretic deposition method. The surface morphology, elemental analysis, crystalline structure, and electrochemical properties of as-prepared nanoSnO 2 -α-Fe 2 O 3 films on titanium substrate surface were characterized by field emission scanning electron microscopy (FE-SEM) with an X-ray spectrometer attached, X-ray diffraction (XRD), linear sweep voltammetry (LSV), cyclic voltammetry (CV), and chrono-potentiometry (CP). The r esults showed that, compared to the traditional nanoSnO 2 electrode, the novel Ti/nanoSnO 2 -α-Fe 2 O 3 electrode with a porous morphology and without voids or cracks on the surface possessed higher electro-catalytic activity and electrochemical stability. To obtain maximum dye removal and t...

中文翻译:

新型Ti / nanoSnO 2-α-Fe2 O 3阳极在染料废水电催化降解中的应用:中央复合设计优化操作参数

在通过阴极电泳沉积法成功制备的新型Ti / nanoSnO 2-α-Fe2 O3电极上研究了酸性黄3染料(AY3)在水溶液中的电化学降解。用X射线光谱仪通过场发射扫描电子显微镜(FE-SEM)表征了钛基体表面制备的nanoSnO 2-α-Fe2 O 3薄膜的表面形貌,元素分析,晶体结构和电化学性能。 X射线衍射(XRD),线性扫描伏安法(LSV),循环伏安法(CV)和计时电位计(CP)。结果表明,与传统的nanoSnO 2电极相比,新型的Ti / nanoSnO 2-α-Fe2 O 3电极具有多孔的形貌,表面无空隙或裂纹,具有较高的电催化活性和电化学稳定性。为了获得最大的染料去除率和色泽
更新日期:2020-06-26
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