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Low-temperature plasma nitriding of martensitic stainless steel
Transactions of the Indian Institute of Metals ( IF 1.5 ) Pub Date : 2020-06-23 , DOI: 10.1007/s12666-020-02013-8
K. Ram Mohan Rao , Corinne Nouveau , K. Trinadh

This study presents the plasma nitriding of Cr–Mo–V tool steel to protect it from environmental degradation. The steel samples after metallographic polishing were nitrided in the glow discharge plasma of N2 and H2 gas mixture (80:20). Nitriding was performed at two different temperatures, a lower temperature of 450 °C and the higher temperature of 500 °C. The potentiodynamic polarization tests in 3.5% NaCl electrolyte had shown the enhancement of corrosion resistance of steels after nitriding. X-ray diffraction (XRD) studies and scanning electron microscopic analysis coupled with energy dispersive spectroscopic analysis (SEM/EDS) was performed to understand the modification of surface microstructure. XRD analysis of the nitrided steels revealed the presence of γ′- and ε-nitrides of iron, which were responsible for the improvement of corrosion resistance.



中文翻译:

马氏体不锈钢的低温等离子体氮化

这项研究提出了Cr-Mo-V工具钢的等离子渗氮处理,以保护其免受环境破坏。金相抛光后的钢样品在N 2和H 2的辉光放电等离子体中氮化混合气体(80:20)。在两个不同的温度下进行氮化,较低的温度为450°C,较高的温度为500°C。在3.5%NaCl电解液中进行的电位动力学极化试验表明,氮化后钢的耐腐蚀性增强。进行了X射线衍射(XRD)研究和扫描电子显微镜分析以及能量色散光谱分析(SEM / EDS),以了解表面微观结构的变化。对氮化钢的XRD分析表明,存在铁的γ'和ε氮化物,这有助于提高耐蚀性。

更新日期:2020-06-23
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