Taking compact NMR to monitoring real reactions in large-scale chemical industries - general considerations and learnings from a lab-scale test case,Magnetic Resonance in Chemistry

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Taking compact NMR to monitoring real reactions in large-scale chemical industries - general considerations and learnings from a lab-scale test case
Magnetic Resonance in Chemistry ( IF 1.9 ) Pub Date : 2020-06-30 , DOI: 10.1002/mrc.5061
Nikolaus Nestle ₁ , Zi Jian Lim ₂ , Tobias Böhringer ₂ , Sarah Abtmeyer ₂ , Sven Arenz ₁ , Felix C Leinweber ₂ , Thomas Weiß ₁ , Erik von Harbou ₃

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The considerations for use of compact NMR in a large-scale industrial environment clearly differ from those in academic and educational settings and even from those in smaller companies. In the first part of this article, these differences will be discussed along with the additional requirements that need to be fulfilled for successful applicability in different use cases. In the second part of the article, outcomes from different research activities aiming to fulfill these requirements will be presented with a focus on an online reaction-monitoring study on a lab-scale nucleophilic chlorination reaction.

中文翻译：

使用紧凑型核磁共振监测大规模化学工业中的真实反应——实验室规模测试案例的一般考虑和学习

在大型工业环境中使用紧凑型 NMR 的考虑明显不同于学术和教育环境中的考虑，甚至与小公司的考虑不同。在本文的第一部分，将讨论这些差异以及在不同用例中成功适用所需满足的其他要求。在文章的第二部分，将介绍旨在满足这些要求的不同研究活动的结果，重点是对实验室规模亲核氯化反应的在线反应监测研究。

更新日期：2020-06-30

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