Abstract—

The characteristic features of the hydrothermal synthesis of molybdenum sulfide nanoparticles, using Na₂MoO₄ as the molybdenum precursor and thioacetamide as the sulfur precursor, at a synthesis temperature of 220°C, and of electrochemical synthesis—anodic formation of nanoparticles from MoS₂ single crystals by electrolysis in an ionic liquid—are described. The X-ray fluorescence, optical absorption, and photoluminescence spectroscopy methods were applied for characterization of the nanoparticles produced.

中文翻译：

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MoS 2纳米粒子的水热和电化学合成及其后期表征

摘要—

以Na ₂ MoO ₄为钼前驱体和硫代乙酰胺为硫前体的水热合成硫化钼纳米粒子的特征温度为220°C，以及电化学合成的特征-单一MoS ₂阳极形成纳米粒子描述了在离子液体中通过电解产生的晶体。X射线荧光，光吸收和光致发光光谱法用于表征所产生的纳米颗粒。