Abstract

The processes and products of the thermal transformations of a chelate complex, bis{N-[2-(allylaminomethyl)phenyl]-4-methylbenzenesulfamidato}copper(II), are studied using thermogravimetry, electron microscopy, microdiffraction of electrons, and IR spectroscopy. The kinetics of the process bears a dispersive character. Depending on the conditions of thermolysis (atmosphere, temperature mode), composite materials filled with copper or copper sulfide nanoparticles are formed as solid products.

中文翻译：

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填充有铜和硫化铜纳米颗粒的复合材料的制备方法

摘要

使用热重分析，电子显微镜，电子微衍射和红外光谱研究了螯合配合物双{ N- [2-（烯丙基氨基甲基）苯基] -4-甲基苯磺酰胺基}铜（II）的热转变过程和产物。。该过程的动力学具有分散性。根据热解的条件（大气，温度模式），形成填充有铜或硫化铜纳米颗粒的复合材料为固体产物。