Abstract

A one-pot method for the synthesis of dipotassium salts of N-alkyl-N-{[O-alkoxy(hydroxy)phosphoryl]methyl}dithiocarbamic acids has been elaborated. Dipotassium salts of N-isopropyl-, N-butyl-, and N-cyclohexyl-N-{[hydroxy(O-ethoxy)phosphoryl]methyl}dithiocarbamic acids as well as N-{[O-butoxy(hydroxy)phosphoryl]methyl}-N-(2-methoxyethyl)dithiocarbamic acid have been synthesized and isolated. Crystal and molecular structure of the latter compound have been elucidated.

中文翻译：

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N-烷基-N-{[O-烷氧基（羟基）磷酰基]甲基}二氨基甲酸二钾盐的合成和晶体结构

摘要

阐述了一种一锅法合成N-烷基-N -{[ O-烷氧基（羟基）磷酰基]甲基}二硫代氨基甲酸二钾盐的方法。的二钾盐Ñ异丙基，Ñ丁基- ，和Ñ环己基Ñ {[羟基（ - ø -乙氧基）磷酰基]甲基}二硫代氨基甲酸以及ñ - {[ ø丁氧基（羟基）磷酰基]甲基} -N-（2-甲氧基乙基）二硫代氨基甲酸已被合成和分离。已经阐明了后一种化合物的晶体和分子结构。