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Preparation and characterization of polyacrylonitrile-based activated carbon nanofibers/graphene (gACNFs) composite synthesized by electrospinning
Aip Advances ( IF 1.4 ) Pub Date : 2020-05-15 , DOI: 10.1063/5.0008012
Faten Ermala Che Othman 1 , Norhaniza Yusof 1 , Ahmad Fauzi Ismail 1 , Juhana Jaafar 1 , Wan Norharyati Wan Salleh 1 , Farhana Aziz 1
Affiliation  

In this work, activated carbon nanofibers (ACNFs) and graphene-derived rice husk (GRH)/ACNF composites (gACNFs) were straightforwardly fabricated through a simple electrospinning process and were consequently activated by using a physical method. The morphological, structural, and textural properties of the resultant ACNFs and (GRH)/ACNFs were characterized by scanning electron microscopy–energy dispersive x-ray spectroscopy, transmission electron microscopy, Raman spectra, thermal gravimetric analysis, and a N2 adsorption isotherm. From the results obtained, gACNFs exhibit better thermal stability properties than pristine ACNFs with improved carbon yield (up to 60%) as well as enhanced adsorption capacity (220 cm3/g). The results including a high specific surface area (592 m2/g) and availability of 80% micropore volumes have demonstrated that gACNFs exhibited double gas adsorption performance as compared to pristine ACNFs.

中文翻译:

电纺合成聚丙烯腈基活性炭纳米纤维/石墨烯(gACNFs)复合材料的制备与表征

在这项工作中,活性碳纳米纤维(ACNFs)和石墨烯衍生的稻壳(GRH)/ ACNF复合材料(gACNFs)通过简单的静电纺丝工艺直接制备,然后通过物理方法进行活化。所得ACNFs和(GRH)/ ACNFs的形态,结构和结构特性通过扫描电子显微镜-能量色散X射线光谱,透射电子显微镜,拉曼光谱,热重分析和N 2吸附等温线表征。根据获得的结果,与原始ACNF相比,gACNF具有更好的热稳定性能,具有更高的碳收率(高达60%)和增强的吸附容量(220 cm 3 / g)。结果包括高比表面积(592 m2 / g)和80%的微孔体积的可用性已证明,与原始ACNFs相比,gACNFs表现出双倍的气体吸附性能。
更新日期:2020-05-15
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