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Synthesis and Structure of 1-Substituted Semithioglycolurils
Synthesis ( IF 2.2 ) Pub Date : 2020-05-25 , DOI: 10.1055/s-0040-1707391 Vladimir V. Baranov 1 , Anton A. Galochkin 1, 2 , Yulia V. Nelyubina 3 , Angelina N. Kravchenko 1, 4 , Nina N. Makhova 1
Synthesis ( IF 2.2 ) Pub Date : 2020-05-25 , DOI: 10.1055/s-0040-1707391 Vladimir V. Baranov 1 , Anton A. Galochkin 1, 2 , Yulia V. Nelyubina 3 , Angelina N. Kravchenko 1, 4 , Nina N. Makhova 1
Affiliation
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Two methods for the synthesis of previously unavailable 1-substituted semithioglycolurils were developed. These methods consist of the cyclocondensation of 1-substituted ureas with 4,5-dihydroxy- or 4,5-dimethoxyimidazolidine-2-thione or glyoxal, followed by the reaction of the resulting 1-substituted 4,5-dihydroxyimidazolidine-2-ones with HSCN in a two-step one-pot procedure. Two of the desired semithioglycolurils were obtained as conglomerates.
中文翻译：
1-取代的半硫甘醇糖醇的合成与结构
开发了两种合成先前不可用的1-取代的半硫甘脲的方法。这些方法包括1-取代的脲与4，5-二羟基-或4，5-二甲氧基咪唑烷-2-硫酮或乙二醛的环缩合，然后使所得的1-取代的4，5-二羟基咪唑烷-2-酮反应。 HSCN采用两步一锅法。获得了两种期望的半硫代糖基尿嘧啶，为团块。
更新日期：2020-05-25
中文翻译：
1-取代的半硫甘醇糖醇的合成与结构
开发了两种合成先前不可用的1-取代的半硫甘脲的方法。这些方法包括1-取代的脲与4，5-二羟基-或4，5-二甲氧基咪唑烷-2-硫酮或乙二醛的环缩合，然后使所得的1-取代的4，5-二羟基咪唑烷-2-酮反应。 HSCN采用两步一锅法。获得了两种期望的半硫代糖基尿嘧啶，为团块。
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