X-ray powder diffraction data for new metal-organic compounds: tetrakis(3-ethylanilinium) octamolybdate Mo8O26(C8H12N)4 [a = 10.682(4), b = 16.589(5), c = 7.307(2) Å, α = 92.79(2)°, β = 97.99(3)°, γ = 103.89(3)°, V = 1240.27 Å3, Z = 1, space group P−1]; tetrakis(3-ethylanilinium) octamolybdate tetrahydrate Mo8O26(C8H12N)4·(H2O)4 [a = 18.801(7), b = 17.943(6), c = 7.334(3) Å, β = 98.50(5)°, V = 2446.99 Å3, Z = 2, space group P21/m] and bis(3-ethylanilinium) pentamolybdate Mo5O16(C8H12N)2 [a = 34.643(6), b = 5.5796(7), c = 14.200(3) Å, β = 96.20(2)°, V = 2728.69 Å3, Z = 4, space group I2/a] are reported in this paper. The investigated compounds were synthesized from molybdic acid and 3-ethylaniline in acidic solution. In the first two cases, we obtained octamolybdates, while the last compound crystallized as pentamolybdate.

中文翻译：

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三种新型 3-乙基苯胺钼酸盐的 X 射线粉末衍射数据

新金属有机化合物的 X 射线粉末衍射数据：四（3-乙基苯胺）八钼酸盐 Mo8○26（C8H12N)4[一种= 10.682(4),b= 16.589(5),C= 7.307(2) 埃，α= 92.79(2)°,β= 97.99(3)°,γ= 103.89(3)°,五= 1240.27 埃3,Z= 1，空间群P-1]; 四(3-乙基苯胺)八钼酸盐四水合物 Mo8○26（C8H12N)4·（H2○）4[一种= 18.801(7),b= 17.943(6),C= 7.334（3）埃，β= 98.50(5)°,五= 2446.99 埃3,Z= 2，空间群磷21/米] 和双（3-乙基苯胺）五钼酸盐 Mo5○16（C8H12N)2[一种= 34.643(6),b= 5.5796(7),C= 14.200(3) 埃，β= 96.20(2)°,五= 2728.69 埃3,Z= 4，空间群一世2/一种] 本文报道。所研究的化合物是由钼酸和 3-乙基苯胺在酸性溶液中合成的。在前两种情况下，我们得到了八钼酸盐，而最后一种化合物结晶为五钼酸盐。