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Quality Dating: A Well-Defined Protocol Implemented at ETH for High-Precision 14C-Dates Tested on Late Glacial Wood
Radiocarbon ( IF 2.0 ) Pub Date : 2019-11-18 , DOI: 10.1017/rdc.2019.132 Adam Sookdeo , Bernd Kromer , Ulf Büntgen , Michael Friedrich , Ronny Friedrich , Gerhard Helle , Maren Pauly , Daniel Nievergelt , Frederick Reinig , Kerstin Treydte , Hans-Arno Synal , Lukas Wacker
Radiocarbon ( IF 2.0 ) Pub Date : 2019-11-18 , DOI: 10.1017/rdc.2019.132 Adam Sookdeo , Bernd Kromer , Ulf Büntgen , Michael Friedrich , Ronny Friedrich , Gerhard Helle , Maren Pauly , Daniel Nievergelt , Frederick Reinig , Kerstin Treydte , Hans-Arno Synal , Lukas Wacker
Advances in accelerator mass spectrometry have resulted in an unprecedented amount of new high-precision radiocarbon (14 C) -dates, some of which will redefine the international 14 C calibration curves (IntCal and SHCal). Often these datasets are unaccompanied by detailed quality insurances in place at the laboratory, questioning whether the 14 C structure is real, a result of a laboratory variation or measurement-scatter. A handful of intercomparison studies attempt to elucidate laboratory offsets but may fail to identify measurement-scatter and are often financially constrained. Here we introduce a protocol, called Quality Dating, implemented at ETH-Zürich to ensure reproducible and accurate high-precision 14 C-dates. The protocol highlights the importance of the continuous measurements and evaluation of blanks, standards, references and replicates. This protocol is tested on an absolutely dated German Late Glacial tree-ring chronology, part of which is intercompared with the Curt Engelhorn-Center for Archaeometry, Mannheim, Germany (CEZA). The combined dataset contains 170 highly resolved, highly precise 14 C-dates that supplement three decadal dates spanning 280 cal. years in IntCal, and provides detailed 14 C structure for this interval.
中文翻译:
质量约会:在 ETH 实施的定义明确的协议,用于在晚期冰川木材上测试的高精度 14C-日期
加速器质谱技术的进步导致了前所未有数量的新型高精度放射性碳(14 C) - 日期,其中一些将重新定义国际14 C 校准曲线(IntCal 和 SHCal)。这些数据集通常没有在实验室提供详细的质量保险,因此质疑这些数据集是否14 C 结构是真实的,是实验室变化或测量分散的结果。少数比对研究试图阐明实验室偏移,但可能无法识别测量分散,并且经常受到财务限制。在这里,我们介绍了一个名为 Quality Dating 的协议,该协议在 ETH-Zürich 实施,以确保可重复和准确的高精度14 C-日期。该协议强调了对空白、标准、参考和复制品进行连续测量和评估的重要性。该协议在绝对过时的德国晚冰期树木年轮年表上进行了测试,其中一部分与德国曼海姆的 Curt Engelhorn 考古中心 (CEZA) 进行了比较。合并后的数据集包含 170 个高分辨率、高精度14 补充三个跨越 280 cal 的年代际日期的 C 日期。IntCal 年,并提供详细的14 此区间的 C 结构。
更新日期:2019-11-18
中文翻译:
质量约会:在 ETH 实施的定义明确的协议,用于在晚期冰川木材上测试的高精度 14C-日期
加速器质谱技术的进步导致了前所未有数量的新型高精度放射性碳(