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Effect of slug flow pattern on supercritical extraction of phenolic compounds from aqueous solutions
The Journal of Supercritical Fluids ( IF 3.4 ) Pub Date : 2020-05-11 , DOI: 10.1016/j.supflu.2020.104885
Peany Houng , Yuya Murakami , Yusuke Shimoyama

This study mainly aims to correlate the effect of high-pressure CO2−Water slug flow formed by microfluidic mixing on the extraction of phenolic compounds (gallic acid, protocetechuic acid, cafeic acid, syringic acid, ferulic acid, and benzoic acid) from its multi-component aqueous solutions. Both slug flow observation and extraction performances were experimentally conducted at different CO2 flow rates (100–650) ml min−1, temperatures (25–60) oC, and pressures (8.0–20.0) MPa. The slug flow patterns are affected by all CO2 flow rates, temperatures, and pressures. The slug flow patterns have a strong correlation with the extraction efficiencies of phenolic compounds from the aqueous solutions. Using slug flow process, benzoic acid can be completely purified from the multi-component aqueous solutions by supercritical CO2 extraction.



中文翻译:

团状流型对水溶液中酚类化合物超临界萃取的影响

这项研究的主要目的是关联微流体混合形成的高压CO 2-水团流对其从中提取酚类化合物(没食子酸,原tech酸,咖啡酸,丁香酸,阿魏酸和苯甲酸)的影响。多组分水溶液。在不同的CO 2流速(100–650)ml min -1,温度(25–60)o C和压力(8.0–20.0)MPa的条件下,均进行了塞流观测和提取性能试验。团状流型受所有CO 2影响流速,温度和压力。团状流型与从水溶液中提取酚类化合物的效率有很强的相关性。使用团流法,可以通过超临界CO 2萃取从多组分水溶液中完全纯化出苯甲酸。

更新日期:2020-05-11
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