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Study on the Magnetic and In Vitro Simulation Targeting Properties of Co 2+ and Dy 3+ Doped Square γ-Fe 2 O 3 Nanoparticles
Journal of Inorganic and Organometallic Polymers and Materials ( IF 3.9 ) Pub Date : 2020-05-02 , DOI: 10.1007/s10904-020-01559-w
Yuxia Guan , Zhaoquan Fei , Tingxin Chen , Guobang Jiang , Weiwei Huan , Xiangnong Liu , Yuxiang Yang , Riccardo Carlini

Pure square γ-Fe2O3 and Co2+, Dy3+ doped γ-Fe2O3 nanoparticles were prepared by coprecipitation method, using ferrous sulfate as the iron source, and anhydrous CoCl2, DyCl3 as doping sources. Nano-magnetic structures and properties were characterized using transmission electron microscopy, X-ray diffraction, X-ray energy dispersive spectroscopy, vibrating sample magnetometer, Mössbauer spectrometer and fluorescence spectrophotometer. Effects of Co2+ and Dy3+ doping amount on their structures, morphologies, magnetic properties and PL properties were discussed. It was found that Co2+ and Dy3+ doped γ-Fe2O3 nanoparticles showed good fluorescent properties and better magnetic properties than pure γ-Fe2O3 with a saturation magnetization at 63.24 emu g−1. Both the 7.56% Co2+ doped and 0.83% Dy3+ doped γ-Fe2O3 reached maximum saturation magnetization at 72.72 and 67.54 emu g−1 respectively. In order to provide a reference for further magnetic targeting drug experiments and animal experiments, the “in vitro” simulation study of magnetic particle targeting in mimetic blood vessels was also carried out.

中文翻译:

Co 2+和Dy 3+掺杂的方形γ-Fe2 O 3纳米粒子的磁和体外模拟靶向特性的研究

纯正方形了γ-Fe 2 ö 3和Co 2+,镝3+掺杂了γ-Fe 2级ö 3通过共沉淀方法制备的纳米粒子,使用硫酸亚铁作为铁源,和无水氯化钴2,DyCl 3作为掺杂源。使用透射电子显微镜,X射线衍射,X射线能量色散光谱,振动样品磁力计,Mössbauer光谱仪和荧光分光光度计对纳米磁性结构和性能进行了表征。讨论了Co 2+和Dy 3+掺杂量对其结构,形貌,磁性能和PL性能的影响。发现Co2+和Dy 3+掺杂了γ-Fe 2个ö 3纳米颗粒表现出良好的荧光特性和更好的磁特性比纯γ-的Fe 2 ö 3在63.24鸸鹋克与饱和磁化强度-1。无论是7.56%的Co 2+掺杂和0.83%的Dy 3+掺杂了γ-Fe 2 ö 3达到最大饱和度在72.72 67.54鸸鹋克磁化和-1分别。为了为进一步的磁性靶向药物实验和动物实验提供参考,还对模拟血管中的磁性粒子靶向进行了“体外”模拟研究。
更新日期:2020-05-02
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