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Furnace for Inelastic X‐Ray Scattering from Liquids up to 1600 °C
Physica Status Solidi (B) - Basic Solid State Physics ( IF 1.5 ) Pub Date : 2020-04-24 , DOI: 10.1002/pssb.202000093
Alfred Q. R. Baron 1 , Masanori Inui 2 , Daisuke Ishikawa 1 , Kazuhiro Matsuda 3 , Yukio Kajihara 2 , Yoichi Nakajima 4 , Kazuhiko Taguchi 1 , Yasunori Hattori 1
Affiliation  

The design and implementation of a furnace for inelastic X‐ray scattering from liquids with sample temperatures up to ≈1600 °C is described. Carbon composite heaters operating in vacuum provide robust heating elements: one pair of heaters has been used for >18 days of operational time above 1500 °C, including eight cycles to room temperature. High‐quality data are obtained to scattering angles as low as 7 mrad in 2θ (Q < 1 nm−1 at 25.7 keV) from a sample at 1560 °C.

中文翻译:

用于从高达1600°C的液体中进行非弹性X射线散射的熔炉

描述了一种用于从样品温度高达1600°C的液体进行非弹性X射线散射的熔炉的设计和实现。在真空中运行的碳纤维复合材料加热器提供了强大的加热元件:一对加热器在1500°C以上的环境下已经使用了18天以上的时间,包括八个室温循环。高品质的数据,得到在2散射角低至7毫弧度θQ  <1个纳米-1 1560从一个样品在25.7千电子伏)℃。
更新日期:2020-04-24
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