Novel Flexible Electrochemical Microreactor and its Validation by Three Model Electrosyntheses,Chemie Ingenieur Technik

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Novel Flexible Electrochemical Microreactor and its Validation by Three Model Electrosyntheses
Chemie Ingenieur Technik ( IF 1.5 ) Pub Date : 2020-04-06 , DOI: 10.1002/cite.201900140
Athanassios Ziogas ₁ , Christian Hofmann ₁ , Sebastian Baranyai _{1,

2} , Patrick Löb ₁ , Gunther Kolb ₁

Affiliation

A novel flexible electrochemical microreactor has been developed. Flexibility is reached by a modular design, suitability for a broad process parameter range including high pressure operation, and accessibility of production scale. Selected reactor aspects have been validated by applying the reactor to three different electrosyntheses: synthesis of tailor‐made mixtures of paraffins by Kolbe electrolysis, cation flow method, and synthesis of peroxodicarbonate. High conversion rates, yields, selectivities, and Faraday efficiency levels have been observed, showing precise process control.

中文翻译：

新型柔性电化学微反应器及其三模型电合成的验证

已经开发了新型的柔性电化学微反应器。模块化设计可实现灵活性，适用于包括高压操作在内的广泛工艺参数范围，并可实现生产规模。通过将反应器应用于三种不同的电合成，已验证了选定的反应器方面：通过Kolbe电解合成量身定制的石蜡混合物，阳离子流方法和过二碳酸酯的合成。已经观察到高转化率，产率，选择性和法拉第效率水平，显示出精确的工艺控制。

更新日期：2020-04-06

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