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Silica gel-coated silicon carbide layer deposited by atmospheric plasma spraying
Journal of the Taiwan Institute of Chemical Engineers ( IF 5.5 ) Pub Date : 2020-04-27 , DOI: 10.1016/j.jtice.2020.04.003
Geng-Sheng Lin , Yu-Cheng Liu , Ramasamy Anbarasan , Keizo Nakagawa , Tomohisa Yoshioka , Hideto Matsuyama , Hui-Hsin Tseng , Kuo-Lun Tung

Atmospheric plasma spraying (APS) of silicon carbide (SiC) is a challenging task due to the severe decomposition behaviour of the SiC. Previous studies, which utilized APS technique, mixed SiC powder with metals and/or metal oxides to prepare SiC coating. None of them sprayed silica gel-coated SiC and examined the characteristics of the coatings. In this work, silica gel-coated SiC, sodium dodecyl sulfate (SDS) enhanced silica gel-coated SiC, and the combination of alumina (Al2O3) and SiC were prepared and then deposited onto a titanium (Ti) plate by APS. Scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD), adhesion and acid resistance test were performed to analyse the characteristics of modified powders and coatings. We found that compared to Commercial-SiC coatings, all the modified SiC coatings not only increase the coating thickness but also enhance the adhesion force between the coating and substrate; furthermore, the SDS-modified sample exhibits good sulfuric acid (H2SO4) resistance. On the other hand, samples containing Al2O3 showed a significant increase in coating thickness and adhesion force, despite a bit lower acid resistance. In sum, we believe that compared to silica-gel coated samples, Al2O3 contained samples are more suitable for industrial application.



中文翻译:

大气等离子喷涂沉积的硅胶涂层碳化硅层

碳化硅(SiC)的大气等离子喷涂(APS)由于SiC的严重分解行为而具有挑战性。先前的研究利用APS技术将SiC粉末与金属和/或金属氧化物混合以制备SiC涂层。他们都没有喷涂硅胶涂层的SiC并检查涂层的特性。在这项工作中,硅胶涂层的SiC,十二烷基硫酸钠(SDS)增强了硅胶涂层的SiC和氧化铝(Al 2 O 3制备SiC和SiC,然后通过APS将其沉积到钛(Ti)板上。进行了扫描电子显微镜(SEM),能量色散X射线光谱(EDS),X射线衍射(XRD),附着力和耐酸性测试,以分析改性粉末和涂料的特性。我们发现,与商品化SiC涂层相比,所有改性SiC涂层不仅增加了涂层厚度,而且增强了涂层与基材之间的附着力。此外,经SDS改性的样品表现出良好的耐硫酸(H 2 SO 4)性能。另一方面,含有Al 2 O 3的样品尽管耐酸性稍低,但涂层厚度和附着力仍显着增加。总而言之,我们认为与硅胶涂层样品相比,包含Al 2 O 3的样品更适合工业应用。

更新日期:2020-04-27
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