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Supercritical antisolvent precipitation of calcium acetate from eggshells
The Journal of Supercritical Fluids ( IF 3.9 ) Pub Date : 2020-04-19 , DOI: 10.1016/j.supflu.2020.104862
Luis C.S. Nobre , Samuel Santos , António M.F. Palavra , Mário J.F. Calvete , Carlos A. Nieto de Castro , Beatriz P. Nobre

The search for sustainable resources remains a matter of global interest. The presence of calcium in food waste may be a material to be valued. In this paper we show a new way of precipitating calcium acetate, produced from eggshells, using the supercritical antisolvent technique (SAS). It also presents the study of the precipitation efficiency as a function of the experimental conditions that affect the SAS results - temperature, pressure, liquid solution concentration and injection flow. It was possible to obtain good results under almost all experimental conditions, highlighting a higher yield for 200 bar pressures and lower solution injection flows. The obtained particles have a rod-like appearance having different sizes depending on the operating conditions.



中文翻译:

超临界反溶剂从蛋壳中沉淀出乙酸钙

寻找可持续资源仍然是全球关注的问题。食物垃圾中钙的存在可能是值得重视的材料。在本文中,我们展示了使用超临界抗溶剂技术(SAS)沉淀从蛋壳中产生的乙酸钙的新方法。还介绍了根据影响SAS结果的实验​​条件(温度,压力,液体溶液浓度和进样流量)对沉淀效率的研究。在几乎所有实验条件下都可能获得良好的结果,突出显示了200 bar压力下的产率更高,溶液注入流量更低。所获得的颗粒具有根据操作条件而具有不同尺寸的棒状外观。

更新日期:2020-04-19
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