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On the role of B4C on hardness and toughness of TiCN - SiC - TiN -Cr3C2 - Co cermet
International Journal of Refractory Metals & Hard Materials ( IF 4.2 ) Pub Date : 2020-03-31 , DOI: 10.1016/j.ijrmhm.2020.105252
Pradhyun Veerapanaicker Soundaraj , Santhosh Sivan Sembulingam , Balasivanandha Prabu Shanmugavel

This paper reports the development of TiCN - SiC- TiN - Cr3C2 - Co cermet modified with B4C for cutting tool applications. Cermets of three different composition with varying B4C in TiCN - SiC - TiN - Cr3C2 - Co were fabricated for a study of addition of B4C on hardness and toughness. The cermet pellets were sintered using Spark Plasma Sintering (SPS) at 50 MPa pressure, 1500 °C temperature at a heating rate of 100 °C/min with 10mins soaking with pulse rate of 12/2 ms. Microstructure examination revealed a typical core-rim structure. Vickers hardness test was done at a load of 30 kg and duration of 10s. Fracture toughness was computed using crack length data measured from the hardness test. The cermet with composition 65% TiCN - 15% SiC - 5% TiN - 5% Cr3C2–10% Co showed high hardness of 16.2 GPa and toughness of 10.7 MPa √m and 50% TiCN - 15% SiC - 5% TiN - 5% Cr3C2–10% Co - 15% B4C exhibited high fracture toughness of 16.5 MPa √m with hardness value of 12 GPa. The addition of B4C greatly enhanced the toughness value and reduced the hardness value slightly.



中文翻译:

B 4 C对TiCN-SiC-TiN -Cr 3 C 2 -Co金属陶瓷硬度和韧性的作用。

本文报道了用切削刀具应用B 4 C改性的TiCN-SiC- TiN-Cr 3 C 2 -Co金属陶瓷的开发。制备了TiCN-SiC-TiN-Cr 3 C 2 -Co中三种不同的B 4 C组成的金属陶瓷用于研究B 4的添加。C关于硬度和韧性。用火花等离子体烧结(SPS)在50MPa压力,1500℃温度下以100℃/ min的加热速率烧结金属陶瓷丸粒,并以12 / 2ms的脉冲速率浸泡10分钟。显微组织检查显示出典型的核心-边缘结构。维氏硬度测试是在30 kg的负载和10s的持续时间下进行的。使用从硬度测试测得的裂纹长度数据计算断裂韧性。成分为65%TiCN-15%SiC-5%TiN-5%Cr 3 C 2 -10%Co的金属陶瓷显示出16.2 GPa的高硬度和10.7 MPa√m的韧性,以及50%TiCN-15%SiC-5%的金属陶瓷TiN-5%Cr 3 C 2 –10%Co-15%B 4C表现出16.5 MPa√m的高断裂韧性,硬度值为12 GPa。B 4 C的添加极大地提高了韧性值,并稍微降低了硬度值。

更新日期:2020-03-31
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