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TCDuino: Development of an Inexpensive Microcontroller-Based Thermal Conductivity Detector for Quantification of Gas Mixtures
Journal of Chemical Education ( IF 2.5 ) Pub Date : 2020-03-31 , DOI: 10.1021/acs.jchemed.9b00977
Bradley A. Owen 1 , Nicholas C. Starvaggi 1 , Taylor I. Mensah 1 , Isaac N. Mills 1
Affiliation  

Thermal conductivity is generally the tool of choice for quantification of fixed gases, particularly lighter-than-air gases. Unfortunately, gas chromatography-thermal conductivity detectors (GC-TCDs) are difficult to introduce in first- and second-year chemistry courses where the cost and number of instruments, as well as the space required, is impractical. In this article, the authors describe the development of a small, inexpensive microcontroller-based TCD for undergraduate teaching and research laboratory experiments which utilizes a matched pellistor pair to quantify hydrogen. The total cost of materials is under $200, including the microcontroller, electronics, TCD pellistor pair, and the mechanical parts which serve as the housing and analysis chamber.

中文翻译:

TCDuino:开发一种基于微控制器的廉价热导率检测器,用于定量混合气体

通常,热导率是定量固定气体(尤其是比空气轻的气体)的首选工具。不幸的是,气相色谱-热导检测器(GC-TCDs)很难在第一年和第二年的化学课程中引入,因为在这些课程中,仪器的成本和数量以及所需的空间都不切实际。在本文中,作者描述了一种小型,廉价的基于微控制器的TCD的开发,该TCD用于本科教学和研究实验室实验,该实验利用匹配的双键对来量化氢。材料的总成本在200美元以下,包括微控制器,电子设备,TCD针对,以及用作外壳和分析室的机械零件。
更新日期:2020-03-31
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