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In Situ Monitoring of Particle Formation with Spectroscopic and Analytical Techniques Under Solvothermal Conditions
Chemical Engineering & Technology ( IF 1.8 ) Pub Date : 2020-04-09 , DOI: 10.1002/ceat.201900520
Heidemarie Embrechts 1, 2 , Martin Hartmann 2, 3 , Wolfgang Peukert 1, 2 , Monica Distaso 1, 2
Affiliation  

The formation of multifunctional materials involves various simultaneous and closely entangled physicochemical processes including nucleation, growth, aggregation, and in some cases also growth by oriented aggregation. These elementary particle formation processes occur in broad size ranges from the molecular to micrometer level and time scales ranging from seconds to hours. This contribution demonstrates that the in situ monitoring of reaction mixtures and dispersions with several simultaneous analytical and spectroscopic techniques is an effective and widely applicable strategy to achieve an in‐depth understanding of the formation of complex particulate structures and to move towards the rational design of materials.

中文翻译:

溶剂热条件下光谱和分析技术对颗粒形成的原位监测

多功能材料的形成涉及各种同时且紧密纠缠的物理化学过程,包括成核,生长,聚集,在某些情况下还通过定向聚集而生长。这些基本的颗粒形成过程以从分子级到微米级的宽范围和从数秒到数小时不等的时间尺度发生。这一贡献表明,使用几种同时进行的分析和光谱技术对反应混合物和分散液进行原位监测是一种有效且广泛适用的策略,可深入理解复杂颗粒结构的形成并朝着合理设计材料的方向发展。 。
更新日期:2020-04-09
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