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Pectin-glycerol gel beads: Preparation, characterization and swelling behaviour.
Carbohydrate Polymers ( IF 10.7 ) Pub Date : 2020-03-13 , DOI: 10.1016/j.carbpol.2020.116166
Fedor V Vityazev 1 , Daria S Khramova 1 , Nikita Y Saveliev 1 , Elena A Ipatova 2 , Andrey A Burkov 3 , Vladislav S Beloserov 3 , Vladimir A Belyi 2 , Leonid O Kononov 4 , Ekaterina A Martinson 3 , Sergey G Litvinets 3 , Pavel A Markov 1 , Sergey V Popov 1
Affiliation  

Low methyl-esterified pectin (AU701) was found to form gel beads with glycerol. Wet AU701-glycerol gel beads exhibited similar diameter and hardness compared to the AU701-Ca gel beads, prepared by ionotropic gelation with Ca2+ and used for comparison. The morphology of dry pectin gel beads determined by scanning electron microscopy revealed that the beads exhibited rough and grooved surface. The AU701-glycerol gel beads absorbed more grams of water than AU701-Ca gel beads (12.2 g vs 3.9 g per 1 g of the beads). Rheological properties and hardness of the AU701-glycerol gel beads improved with the increase of the pectin/glycerol ratio. Swelling behavior of the AU701-glycerol gel beads was determined after sequential incubation in simulated gastric (SGF) and intestinal (SIF) fluids. The AU701-glycerol gel beads swelled in SGF to a greater extent and revealed higher stability in SIF than the gel beads cross-linked by Ca2+.

中文翻译:

果胶甘油凝胶珠:制备,表征和溶胀行为。

发现低甲基酯化的果胶(AU701)与甘油形成凝胶珠。湿AU701-甘油凝胶珠与AU701-Ca凝胶珠相比具有相似的直径和硬度,而AU701-Ca凝胶珠是通过用Ca2 +进行离子凝胶法制备并用于比较的。通过扫描电子显微镜确定的干果胶凝胶珠的形态表明,该珠表现出粗糙且有凹槽的表面。AU701-甘油凝胶珠比AU701-Ca凝胶珠吸收更多的水(每1克珠12.2克比3.9克)。AU701-甘油凝胶珠的流变性质和硬度随果胶/甘油比的增加而提高。在模拟胃液(SGF)和肠液(SIF)中连续孵育后,确定AU701-甘油凝胶珠的溶胀行为。
更新日期:2020-03-16
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