The room-temperature reactions between N-donor ligands 1,3,5-Tris(1H-pyrazol-3-yl)benzene, nickel salts and Succinic acid in hydrothermal processing yielded one new coordination polymer, [Ni(H3tpb)2(Suc)]n⋅nH2O (H3tpb = 1,3,5-Tris(1H-pyrazol-3-yl)benzene, H2Suc = Succinic acid). The coordination polymer has been characterized using single-crystal X-ray diffraction and studied its infrared spectra, elemental analysis, photocatalysis analysis, powder X-ray diffraction analysis. The X-ray structural determination indicates that coordination polymer crystallizes in the monoclinic space group C2/c, with a = 25.929(5) Å, b = 17.831(4) Å, c = 17.717(4) Å, β = 124.65(3), V = 6738(3) Å3.Graphical Abstract

中文翻译：

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镍(II)与1,3,5-三(1H-吡唑-3-基)苯和琥珀酸配位聚合物的合成、结构表征和性能

N-供体配体 1,3,5-Tris(1H-pyrazol-3-yl)benzo、镍盐和琥珀酸在水热处理中的室温反应产生了一种新的配位聚合物，[Ni(H3tpb)2(Suc )]n⋅nH2O (H3tpb = 1,3,5-Tris(1H-pyrazol-3-yl)benzo, H2Suc = 琥珀酸)。采用单晶X射线衍射对配位聚合物进行了表征，并研究了其红外光谱、元素分析、光催化分析、粉末X射线衍射分析。X 射线结构测定表明配位聚合物在单斜空间群 C2/c 中结晶，a = 25.929(5) Å, b = 17.831(4) Å, c = 17.717(4) Å, β = 124.65(3) ), V = 6738(3) Å3.Graphical Abstract