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Characterization of TaC-based fibrous-monolithic ceramics made of fibers with different core/shell volume ratios and orientations
Materials Science and Engineering: A ( IF 6.1 ) Pub Date : 2020-01-08 , DOI: 10.1016/j.msea.2020.138935
Vahideh Shahedifar , Mahdi Ghassemi Kakroudi , Nasser Pourmohammadie Vafa

In this paper, TaC-based/graphite fibrous monolithic ceramics made of fibers with three core/shell volume ratios (75/25, 70/30, and 65/35) and two orientations of 0° and 0°/90° were prepared. Then, the effects of fiber core/shell volume ratio and fiber orientation on the microstructure and room temperature mechanical properties were investigated. Hot pressing at 1800 °C for 60 min under 40 MPa resulted in the maximum relative density for [0°] specimens with the minimum shell thickness. The work of fracture and fracture toughness of FM specimens with 0°/90° fibers orientations were calculated lower than samples with 0° fibers orientations at the same core/shell volume ratio. SEM observations of fracture surfaces and side surfaces of specimens approved these data. So that delamination and fiber pullout occurred in a minimized extent for the specimens with the bi-directional architecture of [0°/90°] compared to the unidirectional architecture of [0°]. The results disclosed that the fracture toughness of 6.6 ± 0.4 MPa m1/2 and work of fracture of 2145 ± 56 J/m2, as the highest values, were obtained for C70/S30-[0°] specimens.



中文翻译:

TaC基纤维整体陶瓷的表征,该陶瓷由具有不同核/壳体积比和方向的纤维制成

本文制备了TaC基/石墨纤维整体陶瓷,该陶瓷由具有三种核/壳体积比(75 / 25、70 / 30和65/35)且两个方向分别为0°和0°/ 90°的纤维制成。然后,研究了纤维核/壳体积比和纤维取向对显微组织和室温机械性能的影响。在40 MPa下于1800°C进行60分钟的热压可得到[0°]标本的最大相对密度,而其外壳厚度最小。计算得出,在相同的核/壳体积比下,纤维取向为0°/ 90°的FM样品的断裂功和断裂韧性低于纤维取向为0°的FM样品。样品的断裂表面和侧面的SEM观察证实了这些数据。因此,与[0°]的双向结构相比,[0°/ 90°]的双向结构的试样在最小程度上发生了分层和纤维拔出。结果表明,断裂韧性为6.6±0.4 MPa m对于C70 / S30- [0°]标本,获得了1/2的最高断裂功和2145±56 J / m 2的断裂功。

更新日期:2020-01-09
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