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Free and hidden fumonisins in raw maize and maize-based products from China.
Food Additives & Contaminants: Part B ( IF 2.9 ) Pub Date : 2019-01-11 , DOI: 10.1080/19393210.2018.1564371
Ling Hu 1 , Hanwei Liu 1 , Jian Yang 2 , Chunfang Wang 1 , Yongjian Wang 1 , Yan Yang 1 , Xianfeng Chen 1
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The occurrence of free and hidden fumonisins in raw maize and maize-based products from China was investigated. A total of 58 samples were analyzed using high-performance liquid chromatography coupled to tandem mass spectrometry (LC-MS/MS). Among all the samples, 66% were contaminated with free fumonisins above limits of quantitation, and a higher percentage of 86% was found for total fumonisins (free + hidden). The highest contamination levels were observed in dried maize kernels which appeared mouldy, with mean levels of 15,737 and 30,785 µg/kg for free and total fumonisins, respectively. Frozen maize kernels, fresh maize kernels, and maize starch samples exhibited the lowest contamination levels, with no more than 200 µg/kg of total fumonisins. Except for one sample, the concentrations of total fumonisins were greater than those of free fumonisins with all the samples, the ratios of total-to-free fumonisins varied between 1.1 and 5.2, with an average ratio of 2.0.

更新日期:2019-01-11
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