Electrochemistry constitutes a mild, green and versatile activation method of organic molecules. Despite these innate advantages, its widespread use in organic chemistry has been hampered due to technical limitations, such as mass and heat transfer limitations which restraints the scalability of electrochemical methods. Herein, we describe an undivided-cell electrochemical flow reactor with a flexible reactor volume. This enables its use in two different modes, which are highly relevant for flow chemistry applications, including a serial (volume ranging from 88 μL/channel up to 704 μL) or a parallel mode (numbering-up). The electrochemical flow reactor was subsequently assessed in two synthetic transformations, which confirms its versatility and scale-up potential.

中文翻译：

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模块化可扩展电化学流动微反应器的设计与应用。


电化学构成了一种温和、绿色、通用的有机分子活化方法。尽管具有这些先天优势，但由于技术限制，例如传质和传热限制，限制了电化学方法的可扩展性，其在有机化学中的广泛应用受到了阻碍。在这里，我们描述了一种具有灵活反应器体积的不可分割的电池电化学流动反应器。这使得它能够以两种不同的模式使用，这与流动化学应用高度相关，包括串行（体积范围从 88 μL/通道到 704 μL）或并行模式（向上编号）。随后在两次合成转化中对电化学流动反应器进行了评估，这证实了其多功能性和放大潜力。